Hi Matt,
Check out MSDN for some great info to start with. http://msdn2.microsoft.com/en-us/library/z9z62c29.aspx http://msdn.microsoft.com/vstudio/teamsystem/support/faqs/profiler_techfaq/
Then I would suggest just running with it and using the tools with your applications and actually checking out what it can do for you.
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